Inert
gas fusion method is used to analyze the material. A small sample of the
material, usually under a gram, is weighed and placed in a graphite crucible.
Next, it is burned in a stream of inert gas. Argon or nitrogen is used for
hydrogen analysis, while helium is used for the oxygen/nitrogen analysis.
Typical
Matrices: Steel-Pins-for-Oxygen-Nitrogen, Chips-for-Carbon-Sulfur-Nitrogen,
Zirconium-Pins-for-Hydrogen-Nitrogen-Oxygen, Steel-Pin-for-Hydrogen, Titanium-Pins-for-Hydrogen-Oxygen-Nitrogen,
Titanium-Zirconium-Pins-for-Hydrogen-Carbon, Copper-Pins-for-Oxygen-Sulfur, Iron-Powders-for-Oxygen-Nitrogen,
Hydrogen-in-Carbon